TOWARD AMPHIPHILIC DIBLOCK COPOLYMERS BY RAFT. KINETIC STUDY ON PH RESPONSIVE POLYMERS
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Reversibleadditionfragmentationtransfer(RAFT)belongstothegroupofthecontrolledradicalpolymerization(CPR)methods,intensivelyemployedinthesynthesisofpolymerswithcomplexarchitecturesandstructures.1,2pHresponsiveamphiphiliccopolymerssynthesizedbyRAFT,leadtomaterialswithversatileproperties.OptimizationofthereactionkineticsduringRAFTpolymerizationof2-(dimethylamino)ethylacrylate(DMAEA)inN,Ndimethylformamide(DMF)wasinvestigatedinthisstudy,followedbythesynthesisofDMAEA/styreneamphiphilicdiblockcopolymers,usingAutomaticContinuousOnlineMonitoringofPolymerizationreactions(ACOMP).Poly(DMAEA)isapHsensitivepolymerwithwideapplicationsinpharmaceuticalandwatertreatmentindustriesyetchallengingduetopossibleinteractionofitsaminogroupwithcatalysts.
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