New Method of Moisture Sensitivity Testing

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2024-09-14 01:08 659阅读次数

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  SuitableanalyzersnTGAThermostepUsedaccessoriesnCeramiccrucible(26063)nSpatula(23111)nQuartzsand(90840)SettingsStepMoisture------------->StepAshnTemperature:105°C600°CnSpeed:0°C(=automatic)0°C(=automatic)nType:StopbydeviationStopbydeviationnTime:0sec0secnDeviation:0.0010.001nGas:NitrogenOxygenFormulasnDrymass:100-((X[0]-(X[1]-Y[1]))/X[0]*100)nAsh(asanalyzed):(X[2]-Y[2])/X[0]*100nAsh(drybase):(X[2]-Y[2])/X[1]*100ProcedurenPrepareandcleantheELTRAanalyzer(e.g.removeashfromthecrucibles)nCheckpressureoftheoxygenandnitrogenbottlenPreparetheapplicationaccordingtotherecommendedsettingsnSelectthisapplicationintheTGAsoftware;loginthesamplenamesandfillapproximately1-2gofquartzsand(90840)intothecruciblesbeforetheweightistakenbytheinternalbalancenSettheoption"BalanceButton"to"Yes"nWhenthecurrentcrucibleisplacedonthepedestalfillinapproximately1gofsamplenRemovethecruciblecarefullyfromtheTGAcarouselandmixthequartzwiththesample(e.g.withaquartztubeorasmallspatula)nPutthecruciblebackonthecarouselandconfirmtheweightbypressingthebalancebutton[详细]

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  SuitableAnalyzersnTGAThermostepUsedAccessoriesn26063ceramiccruiciblenSpatulaSettingsStepMoisture------------->StepCombustion(1)----->StepAshnTemperature:105°C450°C600°CnSpeed:0°C/min0°C/min0°C/minnType:StopbydeviationStopbytimeStopbydeviationnTime:0s01:00:000snDeviation:0.0010.001nGas:NoneNoneOxygenFormulasnMoisture:(X[0]-(X[1]-Y[1]))/X[0]*100nAsh(asanalyzed):(X[3]-Y[3])/X[0]*100nAsh(drybase):(X[3]-Y[3])/X[1]*100ProcedurenPrepareandcleantheELTRAanalyzer(f.e.removeashfromthecruicibles)nCheckpressureoftheoxygenbottlenPrepareonceapplicationaccordingtherecommendedsettingsnSelectthisapplicationintheTGASoftware;Loginthesamplesnamesandfillinthesamples:nELTRArecommendstouse2gofflourforbestrepeatability.[详细]

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  SuitableanalyzersnTGAThermostepUsedaccessoriesnCeramiccrucible(26063)nSpatula(23111)nQuartzsand(90840)SettingsStepMoisture------------->StepAshnTemperature:105°C600°CnSpeed:0°C(=automatic)0°C(=automatic)nType:StopbydeviationStopbydeviationnTime:0sec0secnDeviation:0.0010.001nGas:NitrogenOxygenFormulasnDrymass:100-((X[0]-(X[1]-Y[1]))/X[0]*100)nAsh(asanalyzed):(X[2]-Y[2])/X[0]*100nAsh(drybase):(X[2]-Y[2])/X[1]*100ProcedurenPrepareandcleantheELTRAanalyzer(e.g.removeashfromthecrucibles)nCheckpressureoftheoxygenandnitrogenbottlenPreparetheapplicationaccordingtotherecommendedsettingsnSelectthisapplicationintheTGAsoftware;loginthesamplenamesandfillapproximately1-2gofquartzsand(90840)intothecruciblesbeforetheweightistakenbytheinternalbalancenSettheoption"BalanceButton"to"Yes"nWhenthecurrentcrucibleisplacedonthepedestalfillinapproximately1gofsamplenRemovethecruciblecarefullyfromtheTGAcarouselandmixthequartzwiththesample(e.g.withaquartztubeorasmallspatula)nPutthecruciblebackonthecarouselandconfirmtheweightbypressingthebalancebutton.[详细]

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