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微区取样仪
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2013-07-04 00:00 478阅读次数
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微区取样仪
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微区取样仪
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2013-01-11 00:00
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德国布鲁克微区X射线荧光能谱仪M4 TORNADO
- 小麦元素分布检测-德国布鲁克微区X射线荧光能谱仪M4TORNADOElementalDistributionExaminationonWheatSeedSamplesMeasurementConditionCustomerSampleObjective:ElementaldistributionexaminationofMn,Fe,Zn,Cu,Cd,P,S,Konwheatseedsamples(n=8,bothtransverseandlongitudinalsectionsfor4setsamples),asperreceived.LeftImage:Wheatseedsampleinnon-embedded,longitudinalandtransverseformrespectivelyRightImage:Samples(N=8)LoadingintotheM4SampleChamberAnalysisResult(a)HOSUT2–LongitudinalSectionCameraImage–10xmagnification(Left)andElementalMapping(Right)ofWheatSeedSample“HOSUT2Longitudinalsection”withcombinationofMn,Fe,Zn,Cu,Cd,P,SandKelement.IndividualElementalMappingofZn,FeandMnrespectivelyElementalMappingof(P+S),KandCurespectivelyAnalysisResult(b)HOSUT3–LongitudinalSectionCameraImage–10xmagnification(Left)andElementalMapping(Right)ofWheatSeedSample“HOSUT3Longitudinalsection”withcombinationofMn,Fe,Zn,Cu,P,SandKelement.IndividualPElementalMapping(Left)and“FalseColorDisplay”IndividualPElementalDistributionMapping(Right)onWheatSeed‘HOSUT3–LongitudinalSection’“FalseColorDisplay”:PhosphorusIntensitySaturationcorrelationineachmappingpixel.Forinstance,thered/blackareaiscorrelatedwithlow/nosulfurconcentration;Thephosphoruscontentisfoundhigherinblue/whiteareaascomparedtogreenarea,referringtotheintensitycolorindicatoronrightside.ElementalMappingof(K+S)and(Mn+Fe+Zn)respectivelyConclusionsAsdemonstrated,M4TornadoisabletoperformquickandnondestructivelyelementalmappinganalysisforexaminingvariouselementdistributiononwheatseedSamplesincludingthefollowingcapabilities:1.Highnumberofsamplesloadingatonetimewithlargesamplechamber2.VaryingElementalDistributionStudyincludingP,S,K,Mn,Fe,ZnandCuonwheatseedSamples3.“FalseColorDisplay”functionmodehelpsinelementdistributionexaminationtofurtherextent[详细]
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矿石应用-布鲁克微区X射线荧光
- Stateoftheartmicro-XRFappliedtogeologicalsamplesMicro-XRFongeologicalsamplesM4TornadoLargesamples(H×W×D:200mm×160mm×120mm)Powerfulsamplestage(100mm/s,5kg)Pre-VacuumconditionsfordetectionofelementsdowntoNaPolycapillaryopticsforhighexcitationintensityandspotsize<25μmSDDsfordetection/processingofover100kcpsVariousmeasurementmodes(single-ormulti-point,linescans,areascans)Optional2ndX-raytubeOptional2nddetectorPositionTaggedSpectroscopy(HyperMap)Versatile"data-mining"softwareStandard-freequantificationScanoftheCetaceous/PaleogeneboundaryinRatonBasinUSThinsectionsmeasurements(64-bitOS)TraceelementsingarentThinsectionofagarentcontainingslateFullareamapshowssymmetricMncorewithinthecrystalsSelectedgarnetneasuredextensivelywithstrongprimaryfiltertoreducebackgroundandtoavoidBraggdiffractionpeaks370pixel×460pixel→170000pixelmapMeasurementtime:1s/pixelSteps:25μmSummaryUniquespeedandperfoimanceinthedeterminationoftheelementdistributioninlargesamplewithmeasurementtiomesperpixelof0.3msanduptp4MillionpixelsinasingleHyperMapHighspatialresolutiondownto25μmX-rayspotsize,motorsstepsof4μmOptimalfortheanalysisofinhomogeneoussamples,duetobetteridentificationoftherepresentativelocationofinterestNon-destructive,fastanalysisoflargesampleswithoutpreparation,includingsolid,poweroeliquidsamplesQualitativeandquantitativeanalysisofallelementsfromNaupwards,duetovacuumchamber,detectionlimitforheavytraceelementsinthelowppmrangeStandardlessFundamentalParameterquantificationwithtypecalibrationoptionPowerfulSoftwarewithmultipletoolsforoptimaldatamining[详细]
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2018-08-15 10:57
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