|
Analysis Method |
Product Specification |
Product Result |
|
Chemical Purity by HPLC/UV |
≥98% |
99.95% |
|
Identity by 1H NMR |
Conforms to Structure |
Pass |
|
Identity by 13C NMR |
Conforms to Structure |
Pass |
|
Identity by Mass Spectrometry |
Conforms to Structure |
Pass |
|
Isotope Incorporation by Mass Spectrometry |
≥90% D/Molecule |
93.14%D/Molecule |
|
Intended Use |
|
This material is intended only for laboratory use in analytical and R+D applications. It not suitable for human/animal consumption or for household use. |
|
Hazards |
|
Read Material Safety Data Sheet (MSDS) and understand any potential hazard(s) prior to the use of this product. All chemicals 首ld be considered potentially hazardous in nature and 首ld only be handled by qualified personnel using established good laboratory practices. |
Analytical Data
1. HPLC/UV
|
Instrument: |
Shimadzu LC-20AD |
|
Column: |
Eclipse XDB C18 4.6×250 mm, 5 μm |
|
Mobile Phase: |
A: Water B: Acetonitrile |
|
Gradient: |
A:B(40:60) ,maintain to 21min |
|
Flow Rate: |
1.5 mL/min from 1 min to 10 min 2.0 mL/min from 10 min to 20 min 1.5 mL/min from 20 min to 21 min |
|
Wavelength: |
279nm |
|
Acquisition Date: |
Jul 8th, 2019 |
Peak #
Ret. Time (min.)
Area (mAU)
Height (mAU)
Area %
1
1.811
5383
1204
0.037
2
3.544
2182
311
0.015
3
8.956
14643560
1083460
99.948
Total
14651126
1084975
100.000
2. 1H NMR & 13C NMR
Instrument:
Bruker ANANCE 300MHz
Solvent:
CDCl3
Acquisition Date:
Jul 5th, 2019
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