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求助翻译

1群骚女    2009-05-07    制备液相色谱仪    浏览 669 次

问题一:请问“在GF254硅胶板上,取样点板,在254nm紫外光下观察结果”这句话该如何翻译?ZD是不知道“取样点板”怎么翻译问题二:麻烦高手帮忙翻译一下2Results2.1柱色谱分离结果The... 问题一:
请问 “在GF254硅胶板上,取样点板,在254 nm紫外光下观察结果” 这句话该如何翻译? ZD是不知道“取样点板”怎么翻译

问题二:麻烦高手帮忙翻译一下
2 Results
2. 1 柱色谱分离结果
The results of separation by column chromatography
柱色谱分离过程中,氯仿∶甲醇95∶5和90∶10洗脱出来的流分经过反复的硅胶柱色谱分离纯化得到组分C3。

2. 2 薄层色谱检测结果
The results of Thin-layer chromatography.
组分C3在GF254硅胶板上展开后,可在254nm紫外灯下直观观测为单点,见图1。

2. 3 GX液相色谱分析和制备单体化合物
对组分C3 进行GX液相制备,色谱图显示有4个色谱峰(见图2) ,分离效果较好,收集4个单峰组分,得到4个化合物1~4,对以上4个化合物进行GX液相分析,均为单峰,见图3~4。

3 化合物的结构鉴定
通过制备液相收集得到4个化合物,对其中3个化合物进行结构鉴定:
化合物1, 淡黄色晶体, UV λmax nm (logε) : 248 nm。E IMS,m / z 501. 3 [M + 1 ] + ,分子量为500。化合物1氢谱显示7个甲基信号;δ1. 02, 0. 93, 0. 78 ( each 3H, s) , 0. 89 ( 3H, d, J =6. 4Hz) , 1. 23, 1. 25 ( each 3H, d, J = 5. 2Hz) , 1. 22(3H, s) ,一个连氧碳上的氢信号δ3. 23 (1H, dd, J= 10 Hz) ,符合三萜化合物的结构,可以证明化
合物1为三萜类化合物。
化合物2, UV λmax nm ( logε) : 250 nm。E IMS,m / z 515. 3 [M + 1 ] + ,分子量为514。化合物2的氢谱显示7个甲基信号δ0. 77, 0. 94, 1.01, 1. 22, 1. 23 (3H, s) , 0. 82 (3H, d, 10. 2 Hz) ,一个连氧碳上的氢信号δ3. 22 ( 1H, dd, J = 10. 5Hz) ,一个甲氧基上的氢信号δ3. 66 (3H, s) ,符合三萜化合物的结构,可以证明化合物2为三萜化合物。
化合物3, UV λmax nm ( logε) : 254 nm。EIMS,m / z 531. 2 [M + 1 ] + ,分子量为514。化合物2 的氢谱(见附录)显示7 个甲基信号δ0.78, 0. 82, 0. 87, 1. 03, 1. 24, 1. 31 ( 3H, s) , 1. 17(3H, d, 6. 6 Hz) ,一个乙酰基上的氢信号2. 10(3H, s) ,一个甲氧基团的氢信号3. 68 (3H, s) ,符合三萜化合物的结构,可以证明化合物3为三萜化合物。
化合物4结构较复杂,不能确定是三萜化合物。
二楼的辛苦了,非常感谢你的回答。不过好像没有明白我的意思,而且有google之嫌。

精彩问答
wangbiaocooec 发布日期:2009-05-13
发英文文章难啊,Z好是从相关文献中找差不多的句子套用,要不审稿人一看你就知道是外行,一般的翻译软件这方面没什么用,本人爱莫能助!
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打喷嚏的素面 发布日期:2009-05-10
取样点板:Sampling point board
所有内容:
The question:
I would like to ask "in the GF254 silica gel plate, sampling points, boards, visible under ultraviolet light at 254 nm observed" how to translate this sentence? Focus do not know "sampling points" and how the translation

Second problem: the trouble of translation experts to help you
2 Results
2.1 Separation of the results of column chromatography
The results of separation by column chromatography
Column chromatographic separation process, chloroform: methanol 95:5 and 90:10 pm elution flow out through repeated silica gel column chromatography of the purified components C3.

2.2 Thin Layer Chromatography test results
The results of Thin-layer chromatography.
C3 components on the board in the silica gel GF254 was launched, 254nm UV lamp can be directly observed as a single point, shown in figure 1.

2.3 Preparation of high-performance liquid chromatography analysis and single compounds
Determination of the component C3 to the preparation, chromatogram showed four peaks (see Figure 2), better separation, the collection of four-component single-peak, the four compounds 1 ~ 4, for more than 4 HPLC analysis of compounds are single-peak, see Figure 3 ~ 4.

3 Identification of compounds
Preparation of liquid collected through the four compounds, three of them for structural identification of compounds:
Compounds 1, yellow crystals, UV λmax nm (logε): 248 nm. E IMS, m / z 501. 3 [M + 1] +, molecular weight of 500. 1 H spectrum of compound 7 showed methyl signals; δ1. 02, 0. 93, 0. 78 (each 3H, s), 0. 89 (3H, d, J = 6. 4Hz), 1. 23, 1. 25 (each 3H, d, J = 5. 2Hz), 1. 22 (3H, s), a company's hydrogen-oxygen and carbon signals δ3. 23 (1H, dd, J = 10 Hz), in line with the triterpenoid compounds structure, can prove of
Adduct 1 triterpenes.
Compounds 2, UV λmax nm (logε): 250 nm. E IMS, m / z 515. 3 [M + 1] +, a molecular weight of 514. NMR of compound 2 showed seven methyl signals δ0. 77, 0. 94, 1.01, 1. 22, 1. 23 (3H, s), 0. 82 (3H, d, 10. 2 Hz), a company oxygen and carbon on the hydrogen signal δ3. 22 (1H, dd, J = 10. 5Hz), a hydrogen on the methoxy signal δ3. 66 (3H, s), in line with the structure of triterpenoids, compounds 2 to prove triterpenoids.
Compounds 3, UV λmax nm (logε): 254 nm. EIMS, m / z 531. 2 [M + 1] +, a molecular weight of 514. NMR of compound 2 (see appendix) shows that 7-methyl signal δ0.78, 0. 82, 0. 87, 1. 03, 1. 24, 1. 31 (3H, s), 1. 17 (3H, d, 6. 6 Hz), a hydrogen-acetyl signal at 2. 10 (3H, s), a methoxy-group signal of hydrogen 3. 68 (3H, s), in line with the structure of triterpenoid compounds, can prove compounds 3 triterpenoids.
4 the structure of more complex compounds can not be identified as triterpenoids.
范哲宇sunshine 发布日期:2009-05-09
The question:
I would like to ask "in the GF254 silica gel plate, sampling points, boards, visible under ultraviolet light at 254 nm observed" how to translate this sentence? Focus do not know "sampling points" and how the translation

Second problem: the trouble of translation experts to help you
2 Results
2.1 Separation of the results of column chromatography
The results of separation by column chromatography
Column chromatographic separation process, chloroform: methanol 95:5 and 90:10 pm elution flow out through repeated silica gel column chromatography of the purified components C3.

2.2 Thin Layer Chromatography test results
The results of Thin-layer chromatography.
C3 components on the board in the silica gel GF254 was launched, 254nm UV lamp can be directly observed as a single point, shown in figure 1.

2.3 Preparation of high-performance liquid chromatography analysis and single compounds
Determination of the component C3 to the preparation, chromatogram showed four peaks (see Figure 2), better separation, the collection of four-component single-peak, the four compounds 1 ~ 4, for more than 4 HPLC analysis of compounds are single-peak, see Figure 3 ~ 4.

3 Identification of compounds
Preparation of liquid collected through the four compounds, three of them for structural identification of compounds:
Compounds 1, yellow crystals, UV λmax nm (logε): 248 nm. E IMS, m / z 501. 3 [M + 1] +, molecular weight of 500. 1 H spectrum of compound 7 showed methyl signals; δ1. 02, 0. 93, 0. 78 (each 3H, s), 0. 89 (3H, d, J = 6. 4Hz), 1. 23, 1. 25 (each 3H, d, J = 5. 2Hz), 1. 22 (3H, s), a company's hydrogen-oxygen and carbon signals δ3. 23 (1H, dd, J = 10 Hz), in line with the triterpenoid compounds structure, can prove of
Adduct 1 triterpenes.
Compounds 2, UV λmax nm (logε): 250 nm. E IMS, m / z 515. 3 [M + 1] +, a molecular weight of 514. NMR of compound 2 showed seven methyl signals δ0. 77, 0. 94, 1.01, 1. 22, 1. 23 (3H, s), 0. 82 (3H, d, 10. 2 Hz), a company oxygen and carbon on the hydrogen signal δ3. 22 (1H, dd, J = 10. 5Hz), a hydrogen on the methoxy signal δ3. 66 (3H, s), in line with the structure of triterpenoids, compounds 2 to prove triterpenoids.
Compounds 3, UV λmax nm (logε): 254 nm. EIMS, m / z 531. 2 [M + 1] +, a molecular weight of 514. NMR of compound 2 (see appendix) shows that 7-methyl signal δ0.78, 0. 82, 0. 87, 1. 03, 1. 24, 1. 31 (3H, s), 1. 17 (3H, d, 6. 6 Hz), a hydrogen-acetyl signal at 2. 10 (3H, s), a methoxy-group signal of hydrogen 3. 68 (3H, s), in line with the structure of triterpenoid compounds, can prove compounds 3 triterpenoids.
4 the structure of more complex compounds can not be identified as triterpenoids.
(我把你写的全翻了)
西子湖与颐和园 发布日期:2009-05-08
GF254 silica gel plate in the sampling points, boards, visible under ultraviolet light at 254 nm observations
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