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- 杨小轩09 2014-05-06 00:00:00
- 图3为SiO2、SiO2-NH2和SiO2-N3的红外光谱。所有样品均在1113cm-1处观察到强吸收峰,表明了硅醇基团的Si-O-Si伸缩震动的存在。2926波数的C-H伸缩震动和1456波数的C-H剪式震动表明亚甲基的存在。羟基的伸缩震动和弯曲震动峰分别在1629波数和3600-3300波数处出现。在图3b中,3420波数左右的吸收峰为N-H伸缩震动峰,表明氨基已被引入到SNP的表面。图3c中位于1734波数处的峰是羰基伸缩震动峰。此外,叠氮基修饰的SNP是点击化学的重要中间体,由图3c中在2110波数处新增的峰可得到证明。
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热门问答
- 求高手将下图翻译一下,主要内容应该是红外光谱的分析。
2014-05-05 00:44:33
389
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- 求高手分析红外光谱图
- 如图,纳米氧化铁环糊精聚合乳液,制备方法如下 分别称取:柠檬酸铁10g,三乙醇胺10ml,10gβ-环糊精,吐温40 10ml,司班40 10g,乳化剂OP10ml,石油醚30ml,无水乙醇30ml,MMA单体和环己烷(MMA环己烷质量比为1.2/1.0)的MMMA30g和环己烷25g,去离子水100m... 如图,纳米氧化铁环糊精聚合乳液,制备方法如下 分别称取:柠檬酸铁10g,三乙醇胺10ml,10gβ-环糊精,吐温40 10ml,司班40 10g,乳化剂OP10ml,石油醚30ml,无水乙醇30ml,MMA单体和环己烷(MMA环己烷质量比为1.2/1.0)的MMMA30g和环己烷25g,去离子水100ml加入到250ml的三口烧瓶中,搅拌,水浴加热,在65~85℃之间恒温回流3小时,冷却至室温,加三乙醇胺调节PH值(PH=6~8),然后水浴加热使每分钟上升0.5℃至65℃,再恒温回流1小时。冷却至室温离心分离(5min,5000r/min)后减压过滤得棕黄色的乳液,有刺激性气味,放入85~100℃的烘箱中24小时除去石油醚及无水乙醇。 现得到其红外光谱图,不知道如何分析,请高手赐教 如果回答好,另外加分,谢谢 展开
2010-05-23 13:47:21
295
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- 英语高手帮忙翻译一下
- ThequalitysystemofthecompanyisinconformitywithISO9002.Makingcomprehensiveuseofbiotechnology,thecompanyspecializesinmanufacturingandsellingC-4seriesorganicacidsandchiralpr... The quality system of the company is in conformity with ISO 9002 . Making comprehensive use ofbiotechnology, the company specializes in manufacturing and selling C-4series organic acids and chiral products. These products are widely used in many fields such as food, phamaceutical and chemical industries, and are well accepted by the overseas markets. The man products are L-Malic acid , DL-Malic acid, L(+)-Tartaric acid , Fumaric acid, Maleic acid and other organic acids. Annual productivity amounts to 20,000 tones. The company has become an important manufacturer of C-4 series organic acids in the world . All the products of the company have respectively met the different international aadvanced standards such as Food chemicals Codex, U.S. Pharmacopoeia ,British Pharmacopoeia and the products have obtained Star-K Kosher certificate. Above 70% of the Companys products are exported to Japan, Europe, Australias, the United states and middle East , and they are renown and well recognized in the international markets. The company will devote itself to research and development of enzyme technology and organic electrochemistry. It will continuously introduce new food additives, chiral pharmaceutical intermediates, chiral auxiliaries and chiral drugs. Depending on superior quality, good service and high reputation, the company is willing to establish a long-term mutually beneficial business partnership with overseas customers and continue contribute to the happy life of humans. 展开
2009-09-17 10:19:02
513
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- 50分!高手帮忙翻译一下
- LabVIEWisapowerfulandcomplexprogrammingenvironment.LabVIEWisshortforLaboratoryVirtualInstrumentEngineeringWorkbench.Itisapowerfulandflexibleinstrumentationandanalysissoft... LabVIEW is a powerful and complex programming environment. LabVIEW is short for Laboratory Virtual Instrument Engineering Workbench. It is a powerful and flexible instrumentation and analysis software development application created by the folks at National Instruments—a company that creates hardware and software products that leverage computer technology to help engineers and scientists take measurements, control processes, and analyze and storem data. National Instruments was founded over twenty-five years ago in Austin, Texas by James Truchard (known as Dr. T), Jeffrey Kodosky, and William Nowlin. At the time, all three men were working on sonar applications for the U.S. Navy at the Applied Research Laboratories at The University of Texas at Austin. Searching for a way to connect test equipment to DEC PDP-11 computers, Dr. T decided to develop an interface bus. He recruited Jeff and Bill to join him in his endeavor, and together they successfully developed LabVIEW and the notion of a “virtual instrument.” In the process they managed to infuse their new company—National Instruments—with an entrepreneurial spirit that still pervades the company today. Engineers and scientists in research, development, production, test, and service industries as diverse as automotive, semiconductor, aerospace, electronics, chemical, telecommunications, and pharmaceutical have used and continue touse LabVIEW to support their work. LabVIEW is a major player in the area of testing and measurements, industrial automation, and data analysis. For example, scientists at NASA’s Jet Propulsion Laboratory used LabVIEW to analyze and display Mars Pathfinder Sojourner rover engineering data, including the position and temperature of the rover, how much power remained in the rover’s battery, and generally to monitor Sojourner’s overall health. LabVIEW provides an extensive library of virtual instruments and functions to help you in your programming. It includes conventional program debugging tools with which you can set breakpoints, single-step through the program, and animate the execution so you can observe the flow of data. 毕业设计急用,望高手帮忙翻译一下 展开
2007-06-12 15:44:11
618
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- 翻译翻译,请高手帮我翻译一下这个说明
- Followthesysteminstallationinstructionscarefullyandinthespecifiedorder.ThesoftwaremustbeinstalledonthecomputerbeforeconnectingtheUSBcable.2.1FacilitiesRequirementsFacilit... Follow the system installation instructions carefully and in the specified order. The software must be installed on the computer before connecting the USB cable. 2.1 Facilities Requirements Facilities requirements for the alpha-SE system are listed in Table 2-1 and the system dimensions are given in Fig. 2-1. As shown in Fig. 2-2, the alpha-SE tool requires a clear work area of 20 by 18 inches (500 by 460 mm), excluding the operator computer. 2.2 Unpacking the Hardware Opening the Shipping Container Move the alpha-SE shipping container to the area where the tool will be installed. Open the container and remove the top and side pieces of packing foam. Carefully remove all smaller components from the shipping container, verifying that you received all components, as shown in Fig. 2-3. Finally, remove the alpha-SE ellipsometer and position it on your clear 20” by 18” (510 by 460 mm) workspace. Caution: The alpha-SE ellipsometer without sample chuck weighs approximately 37 lbs. (16 kg.). Please find an assistant to lift the alpha-SE unit out of the shipping carton and on to clear work surface. 展开
2008-06-22 06:30:36
788
4
- 高分求高手翻译,不要机械翻译
- Bimetallic dendrimer-encapsulated nanoparticles(DENs)are important materials,because they have demonstrated improvement in performance compared to the monometallic DENs in many systems when they are used as catalysts.This tutorial review fo... Bimetallic dendrimer-encapsulated nanoparticles(DENs)are important materials,because they have demonstrated improvement in performance compared to the monometallic DENs in many systems when they are used as catalysts.This tutorial review focuses on the recent research advances in bimetallic DENs with respect to their synthesis,characterization,and applications as catalysts.Bimetallic DENs can be made mainly via three routes:co-complexation,sequential loading,and partial displacement.The research in bimetallic DENs has been significantly promoted by the advancement of characterization instruments.The performances of bimetallic DENs as homogeneous and heterogeneous catalysts in organic synthesis have been compared with both monometallic DENs and their physical mixtures.It is concluded that the synergistic electronic effect in bimetallic nanoparticles enhances their catalytic activities. 能翻译多少都可以的 展开
2009-03-24 13:04:22
309
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- 请高手帮我翻译一下这一段。。。
- Carbonnanomaterialsarenovelmanufacturedmaterials,havingwidespreadpotentialapplications.Adsorptionofhydrophobicorganiccompounds(HOCs)bycarbonnanomaterialsmayenhancetheirto... Carbon nanomaterials are novel manufactured materials, having widespread potential applications. Adsorption of hydrophobic organic compounds (HOCs) by carbon nanomaterials may enhance their toxicity and affect the fate, transformation, and transport of HOCs in the environment. In this research, adsorption of naphthalene, phenanthrene, and pyrene onto six carbon nanomaterials, including fullerenes, single-walled carbon nanotubes , and multiwalled carbon nanotubes was investigated, which is the first systematic study on polycyclic aromatic hydrocarbons (PAHs) sorption by various carbon nanomaterials. All adsorption isotherms were nonlinear and were fitted well by the Polanyi-Manes model (PMM). Through both isotherm modeling and constructing “characteristic curve”, Polanyi theory was useful to describe the adsorption process of PAHs by the carbon nanomaterials. The three fitted parameters (Q0, a, and b) of PMM depended on both PAH properties and the nature of carbon nanomaterials. For different PAHs, adsorption seems to relate with their molecular size, i.e., the larger the molecular size, the lower the adsorbed volume capacity (Q0), but higher a and b values. For different carbon nanomaterials, adsorption seems to relate with their surface area, micropore volume, and the volume ratios of mesopore to micropore. Quantitative relationships between these sorbent properties and the estimated parameters of PMM were obtained. These relationships may represent a first fundamental step toward establishing empirical equations for quantitative prediction of PAH adsorption by carbon nanomaterials and possibly other forms of carbonaceous (geo-) sorbents, and for evaluating their environmental impact. In addition, high adsorption capacity of PAHs by carbon nanotubes may add to their high environmental risks once released to the environment, and result in potential alteration of PAHs fate and bioavailability in the environment. 展开
2010-01-13 13:35:43
309
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- 请高手帮忙翻译一下 3
- 2.2.1. Physical and physicochemical characterization The particle size distribution of the Ch-zeolite was determined using a laser diffraction equipment (CILASk 1064) and standard wet sieving (Mesh Tylerk series). Scanning electron mic... 2.2.1. Physical and physicochemical characterization The particle size distribution of the Ch-zeolite was determined using a laser diffraction equipment (CILASk 1064) and standard wet sieving (Mesh Tylerk series). Scanning electron microscopy (SEM-PHILIPSk XL20) was used for photomicrographs as well as to analyse the Ch-zeolite composition (Energy Dispersion X-ray, EDX). The sample was initially placed in a vacuum chamber for coating with a thin layer (few nanometers) of gold (Au). The specific surface area of the material was measured by the methylene blue technique and by nitrogen gas adsorption methods, with the latter also providing information about particle porosity. In the methylene blue adsorption method, aqueous solutions (50 ml) of methylene blue (100 mg l 1) were agitated using an orbital shaker (Marconik) for an hour at room temperature in the presence of different quantities of the Ch-zeolite (0.05–0.3 g). The suspensions were then allowed to settle for 23 h and the resulting supernatants were centrifuged at 5000 rpm before the analysis of the residual methylene blue concentration. Results obtained correspond to averaged values of three different experiments. The specific surface area was evaluated by the Langmuir model, assuming the formation, at high concentrations, of a dye monolayer and 1.08 nm2 molecule 1, for the cross-sectional area (Van den Hul and Lyklema, 1968). The Ch-zeolite specific surface area was evaluated by the nitrogen gas adsorption method, using automated equipment (Autosorb 1-Quantachrome Instrumentsk), employing multipoint BET isotherm adsorption data fitting. Also from these data, the porosity of the material was evaluated through parameters such as volume of total pores (d < 206 nm), surface area and volume of micropores (d < 2 nm; Micropore Analysis Method). Zeta potential measurements for the natural and ammonia loaded zeolite, as a function of medium pH, were determined using a Zeta Plusk equipment (Brookhaven Instruments). Suspensions (0.01% v/v) of the Ch-zeolite, previously sieved below 37 Am (400 Mesh Tylerk), in a 10 3 mol l 1 solution of KNO3 were used and the medium pH was controlled with the addition of HNO3 (pH< 7) and KOH (pH>7), separately. For the Ch-zeolite saturated with ammonia, suspensions of the material were prepared by the same procedure, except that the sample was loaded with 100 mg NH3–N l 1 of ammonia. 展开
2018-11-22 17:49:22
256
0
- 做质谱的高手帮忙翻译一下
- 下面是做气相质谱给出的参数,用的机子是:珀金埃尔默(perkinElmer)Clarus500GC/MS。拜托各位帮忙翻译一下,谢谢Inst()ACQUISITIONPARAMETERSOven:Initialtemp35°Cfor2min,ramp10°... 下面是做气相质谱给出的参数, 用的机子是:珀金埃尔默(perkin Elmer)Clarus 500 GC/MS。 拜托各位帮忙翻译一下,谢谢 Inst() ACQUISITION PARAMETERS Oven: Initial temp 35°C for 2 min, ramp 10°C/min to 150°C, hold 2.50 min, InjAauto=150°C, Volume=0 µL, Split=35:1, Carrier Gas=He, Solvent Delay=0.10 min, Transfer Temp=280°C, Source Temp=260°C, Scan: 5 to 300Da, Column 30.0m x 250µm 展开
2008-10-25 00:03:10
597
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- 英文高手帮忙翻译一下 压力容器方面
- 公司接到一个压力容器图纸是英文版的想知道其中的一些意思,原文如下:一TECHNICALDATA:1.MAXIMUMALLOWABLEPRESSURE7.0BAR2.WORKINGPRESSURE5.5+/-1.0BAR3.TESTPRESSURE10.0BAR4.MAXI... 公司接到一个压力容器图纸 是英文版的 想知道其中的一些意思,原文如下: 一 TECHNICAL DATA: 1.MAXIMUM ALLOWABLE PRESSURE 7.0BAR 2.WORKING PRESSURE 5.5+/-1.0BAR 3.TEST PRESSURE 10.0BAR 4.MAXIMUM ALLOWABLE TEMPERATURE 70℃ 5.MINIMUM ALLOWABLE TEMPERATURE 0℃ 6.FLUID PREFILL(ISO VG46-HLP) 7.CORROSION ALLOWABLE 2mm 8.VOLUME 38.00L 二 TECHNICAL ACCEPTANCE: 1.CHINA DECLARATION OF CONFORMITY 2.CONFORITY ASSESSMENT PROCEDURE REPORTS 3.BILL OF MATERIALS 4.INSPECTION DOCUMENTS AND CERTIFICATES FOR USED MATERIALS 5.WELDING MAP 6.LIST OF WELDERS AND THEIR QUALIFICATION CERTIFICATES 7.NDE EXAMINATION REPORTS 8.VT AND MEASUREMENT REPORTS 9.PAINT: EXTERNAL:BLUE RAL 5015 SEMI-GLOSS FINISH INTERNAL:USE SUNCORITE 528 BY HENKEL METAL CHEMICALS TO TREAT INTERNAL SURFACE OF TANK 10.PAINT REPORT 11.TECHNICAL DOCUMENTATION AND OPERAING MANUAL 三 NOTES: 1.ALL DIMENSIONS ARE IN MILLIMETER UNLESS OTHERWISE NOTED. 2.GASKET CONTACK SURFACE OF ALL FLANGES SHALL BE FINISHED WITH 125-250 AARH. 3.INTERNAL WELD SURFACE OF INSTRUMENT NOZZLE TO BE FULLY FLUSHED. 4.PAINT INSIADE AND OUT PER OILGEAR STANDAR SOP-U-002. 5.TATAL WEIGHT OF UNIT ASSEMBLY IS 32,900LB[14,900kg]. 6.DIMENSIONS IN MM. 展开
2010-07-15 11:42:12
559
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- 跪求(急求)帮忙翻译一下
- 无机前处理室主要开展食品样品中无机检测进仪器前的预处理工作。通过向食品样品中加入强氧化性酸,采用微波消解技术或电热板加热技术使被测无机组分从复杂的样品中分离出来,除去对分... 无机前处理室主要开展食品样品中无机检测进仪器前的预处理工作。通过向食品样品中加入强氧化性酸,采用微波消解技术或电热板加热技术使被测无机组分从复杂的样品中分离出来,除去对分析测定有干扰的基本物质,制成便于测定的溶液形式。样品的预处理过程都是在无机前处理室进行的。 主要仪器:ETHOS A微波消解仪、SD500电热板、Mill-Q Advandage A10超纯水仪等。 光谱室主要开展食品、饮用水等样品中重金属元素含量检测工作,各类仪器针对不同的物质进行检测有其各自的优势。原子吸收光谱仪耶拿ZEEnie-700系列仪器主要用于铅、镉、铜、铬、锰、锌、铁、钙、镁、钾、钠等项目检测,双道原子荧光光度计吉天AFS-820a系列仪器主要用于砷、汞、锡等项目检测。光谱分析技术已经被广泛应用于食品和水质检测、环境保护、医药卫生等领域。 主要仪器:原子吸收光谱仪耶拿ZEEnie-700系列、双道原子荧光光度计AFS-820a系列。 承检项目:食品、饮用水中重金属铅、镉、铜、铬、锰、锌、铁、钙、镁、钾、钠、砷、汞、锡等。 要英文的谢谢 展开
2013-02-18 02:23:38
300
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- 哪位高手能帮我翻译一下 谢谢了
- 3.3. Microbial mapping The intensity of resonance Raman spectra of Cyt c allows for integration times below one second. Microbial mapping of an area of 50×50 μm2 with a resolution of 500 nm/pixel (10,000 single spectra) can be perform... 3.3. Microbial mapping The intensity of resonance Raman spectra of Cyt c allows for integration times below one second. Microbial mapping of an area of 50×50 μm2 with a resolution of 500 nm/pixel (10,000 single spectra) can be performed in less than 3 h. A further reduction of the measuring duration by a factor of 10 can be achieved by utilisation of an EMCCD camera (Coates et al., 2004). Microbial mapping was done on granules from two different sequencing batch reactors (SBR) (Gaul et al., 2006). The SBRs are used to analyse control parameters for the anaerobic ammonium oxidation. Fig. 7 shows two different microbial colonies in the same granulum. A graphical analysis of the spectroscopic data at 750 cm-1 (dominant resonant Raman band of Cyt c) and 2900 cm-1 (CH stretching mode) differentiated the two colonies. One colony shows stronger Raman signals at 750 cm-1 (blue frame). Whereas the other microorganisms have more amount of methyl or methylene groups (yellow frame). After the graphical analysis above, an average spectrum was constructed for each colony. The resulting averaged spectra were transferred to our Raman database of wastewater bacteria created by OPUS. The software recognized the microorganisms Fig. 5. Time series of N. eutropha Nm 57 which is captured by optical tweezers. Time difference between spectra: 1 s; Laser power: 9 mW. The bleaching effect due to photo-dissociation caused by laser radiation is easy to see. Fig. 6. The spectral heterogeneity of hierarchical clusteringis strongly dependent to the integration time. Bacteria from the same strain are only groupedtogether if the exposure time was the same. 246 R. P?tzold et al. / Journal of Microbiological Methods 72 (2008) 241–248 in the left colony as anammox bacteria, those in the upper right corner as Nitrosomonas. 展开
2008-11-08 00:52:54
380
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- 求日语 日文翻译帮忙翻译一下。。。万分感谢
- 请求项2记载の透明硬脆材料のレーザ加工装置において、前记半透过ミラー及び前记反射ミラーにおける凹面のそれぞれの焦点位置が、同位置となるよう配置したことを特徴とするレーザ加工装置。
2014-03-16 13:43:20
574
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- 急求分析红外光谱图
- 红外光谱分析,3403cm-1 (强吸收),3257.40cm-1,1662cm-1,1088cm-1(强吸收),976cm-1(弱),748cm-1,615cm-1(较强),423cm-1 以上是我做的一种物质的红外吸收,请高人帮分析一下这是什么物质,万分感谢!
2012-11-25 07:41:43
243
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- 请高手翻译一下有关测量设备的日语说法
- 低温脆性试验机. 硫变仪. 门尼仪. 垂直弹性仪. 电击穿试验机. 压缩弹性仪 AKRON耐磨耗试验机 换气式热空气老化箱 这些设备用日语怎么说啊,请帮帮忙啊,谢谢
2010-06-27 19:53:21
521
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- 宏观分析 指标分析的主要内容
2011-12-18 09:34:07
335
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- 帮忙翻译一下,求速度,考试中
- 题目是:aboutvirtualinstrumentation!内容各位大神自己百度吧,手机不方便了。翻译全文没事,Z好附原文。原文diyi句是WITHmorethan6……应该够了哈,有道,谷歌翻译的就成了,麻烦... 题目是:about virtual instrumentation!内容各位大神自己百度吧,手机不方便了。翻译全文没事,Z好附原文。原文diyi句是WITH more than 6……应该够了哈,有道,谷歌翻译的就成了,麻烦速度! 发这个邮箱吧,122524007@qq.com! 展开
2011-05-29 01:56:08
408
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