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请帮我翻译下下边几句话,十分感谢, 跪求通顺语句 给分

changshengwei7 2011-06-06 02:19:24 331  浏览
  • 以烷基酚(AP)为目标分析物,用1:1(V/V)甲醇水溶液溶解,调pH=2~3,离心后过C18柱固相萃取,以正己烷洗脱,去除水层,在60℃下氮吹干,与衍生剂在90℃下反应30min,用GC-MS分析测... 以烷基酚(AP)为目标分析物,用1:1(V/V)甲醇水溶液溶解,调pH=2~3,离心后过C18柱固相萃取,以正己烷洗脱,去除水层,在60 ℃下氮吹干,与衍生剂在90 ℃下反应30 min,用GC-MS分析测定。以烷基酚聚氧乙烯醚(APEO)为目标分析物,样品直接溶解于甲醇后离心,真空抽取至近干后用甲醇洗涤收集,旋转蒸发浓缩至近干后转入容量瓶中定容之,取一定量用有机膜离心过滤, 用液相色谱与液质结合测定。AP的回收率在 85.2 %~109.7 % 之间,精密度在 2.27 %~6.57 % 之间(n=5);APEO的回收率在85.3 %~108.1 % 之间,精密度在2.68 %~5.95 %(n=5)。 展开

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  • 户神翼33 2011-06-20 00:00:00
    To alkylphenols (AP) for the target analyte, with 1:1 (V / V) aqueous methanol solution, adjust pH = 2 ~ 3, after centrifugation through C18 SPE column, eluting with hexane to remove the water layer, dry nitrogen at 60 ℃, and the derivative agent at 90 ℃ for 30 min, determined by GC-MS analysis. To alkyl phenol ethoxylates (APEO) for the target analyte, dissolved in methanol directly after sample centrifugation, vacuum extraction to nearly dry after washing with methanol, collected, rotary evaporation to near dried into a constant volume of the flask, take a certain amount of organic membrane centrifugal filtration, liquid chromatography and liquid chromatography combined with determination. AP recoveries between 85.2% ~ 109.7%, precision at between 2.27% ~ 6.57% (n = 5); APEO recoveries between 85.3% ~ 108.1%, precision 2.68% 5.95% (n = 5). 你看看觉得怎么样

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  • 一米阳光_1225 2011-06-09 00:00:00
    起码10分,不然只有机译版,有语法错误,通顺是不可能的了

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  • 巍澜北居 2011-06-07 00:00:00
    The alkylphenols (AP) as the target analyte, with 1:1 (V / V) aqueous solution of methanol, adjusting pH = 2 ~ 3, after centrifugation through C18 solid phase extraction column, eluting with hexane to remove the water layer, dry nitrogen at 60 ℃, and the derivatized reaction at 90 ℃ for 30 min, determined by GC-MS analysis. The alkylphenol ethoxylates (APEO) for the target analyte, the sample was dissolved in methanol directly after the centrifugation, vacuum extraction to nearly dry after washing with methanol to collect, rotary evaporation to near dried into a constant volume of the flask, take a certain amount of organic membrane centrifugal filtration, using liquid chromatography and liquid chromatography combined with determination. AP recovery rate 85.2% to 109.7%, precision at between 2.27% ~ 6.57% (n = 5); APEO recoveries between 85.3% ~ 108.1%, precision 5.95% 2.68% (n = 5).

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请帮我翻译下下边几句话,十分感谢, 跪求通顺语句 给分
以烷基酚(AP)为目标分析物,用1:1(V/V)甲醇水溶液溶解,调pH=2~3,离心后过C18柱固相萃取,以正己烷洗脱,去除水层,在60℃下氮吹干,与衍生剂在90℃下反应30min,用GC-MS分析测... 以烷基酚(AP)为目标分析物,用1:1(V/V)甲醇水溶液溶解,调pH=2~3,离心后过C18柱固相萃取,以正己烷洗脱,去除水层,在60 ℃下氮吹干,与衍生剂在90 ℃下反应30 min,用GC-MS分析测定。以烷基酚聚氧乙烯醚(APEO)为目标分析物,样品直接溶解于甲醇后离心,真空抽取至近干后用甲醇洗涤收集,旋转蒸发浓缩至近干后转入容量瓶中定容之,取一定量用有机膜离心过滤, 用液相色谱与液质结合测定。AP的回收率在 85.2 %~109.7 % 之间,精密度在 2.27 %~6.57 % 之间(n=5);APEO的回收率在85.3 %~108.1 % 之间,精密度在2.68 %~5.95 %(n=5)。 展开
2011-06-06 02:19:24 331 3
急!!!谁能帮我翻译一下?万分感谢!
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2008-06-22 06:30:36 798 4
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2010-12-10 08:46:08 478 2
谁能帮我翻译下这片文章?翻译的好的在追加100分!!!
Experimental Method All experiments were carried out in a high-pressure CO2 apparatus (Speed-SFE from Applied Separations) (see Figure 1) with a 300-mL extractor designed for a maximum pressure of 690 bar and a maximum temperature of 2... Experimental Method All experiments were carried out in a high-pressure CO2 apparatus (Speed-SFE from Applied Separations) (see Figure 1) with a 300-mL extractor designed for a maximum pressure of 690 bar and a maximum temperature of 250 °C. The volume of the extractor had to be reduced to 50 mL by a metallic cylinder, which tightens to the extractor wall, because as preliminary tests showed the equilibrium cell has to be completely filled with material. Otherwise, diffusion is the limiting factor and time for reaching equilibrium was too long. The extraction vessel was filled with compressed CO2 by an air-driven pump at closed outlet valves and under static conditions, which means desired pressure and temperature; the cell was incubated for 15 h, maintaining these conditions to reach equilibrium. In preliminary experiments the equilibrium time of 15 h was determined to reach equilibrium. CO2 Sampling. At equilibrium a CO2 phase sample is taken by opening the outlet valve and expanding a certain amount of CO2-substance mixture into a cooling trap filled with toluene, which has the highest solubility for the measured substances under atmospheric conditions. The pure gaseous CO2 passes a rotameter, showing the actual flow rate, and a gas flowmeter for determining the expanded CO2 amount. The content of the cooling trap was filled up with toluene to 30 mL and analyzed by a gas chromatographic method using an electron capture detector (GC-ECD). With the mass of expanded CO2 and composition of the cooling trap solubility at a certain pressure and temperature was calculated. Sampling was repeated four times at a given pressure and temperature and the standard deviation was lower than 5%. Gas Chromatographic Method. The tolueneflame retardant mixture of CO2 sampling was analyzed in a gas chromatograph (HP 5890 Serie II) with an ECD using a capillary column (type HP-1, 12 m  0.2 mm  0.2 ím). The injector temperature was held constant at 290 °C and the detector temperature at 300 °C. The oven temperature was held constant at 290 °C. Calibration with different amounts of HBCD and TBBA in toluene has been done before determining the linear range of calibration line and retention time of substances 展开
2008-06-04 17:17:07 504 1
请英语高手帮我翻译下面盐雾测试报告里面部分内容
1 外观评级,试样表面外观的变化. 2 腐蚀率评定等级的判定等级的判定腐蚀率. 3 无变化. 4 轻微到中度的变色. 5 严重变色到极微的失光. 6 轻微的失光或出现极轻微的腐蚀产物. 7 严重失光或在试样局部表面上部有薄层的腐蚀产物或点蚀. 8 有腐蚀物或点蚀且... 1 外观评级,试样表面外观的变化. 2 腐蚀率评定等级的判定等级的判定腐蚀率. 3 无变化. 4 轻微到中度的变色. 5 严重变色到极微的失光. 6 轻微的失光或出现极轻微的腐蚀产物. 7 严重失光或在试样局部表面上部有薄层的腐蚀产物或点蚀. 8 有腐蚀物或点蚀且其中之一集中分布在整个试样表面上. 9 整个表面上布有厚的腐蚀产物,并有深的点蚀. 10 整个表面布有非常厚的腐蚀物和点蚀,并有深的点蚀. 11 出现基体金属腐蚀. 展开
2007-09-05 04:44:20 429 1
帮我翻译下8种有机锡化物的名字! 谢谢 !
帮我翻译下8种有机锡化物的名字!谢谢!Monobutyltin/Monooctyltin/Dibutyltin/Dioctytlin/Triphenyltin/Triphenyltin/Tricyclohexyltin/Tetrabutyltin.... 帮我翻译下8种有机锡化物的名字! 谢谢 !Monobutyltin/Monooctyltin/Dibutyltin/ Dioctytlin/Triphenyltin/Triphenyltin/Tricyclohexyltin/Tetrabutyltin. 展开
2009-07-21 06:25:05 565 1
罗茨泵操作规程,要详细的谁有,十分感谢。
2014-11-13 22:18:10 459 1

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